Inorganic Syntheses, Volume 20
John Wiley & Sons, Sep 22, 2009 - Science - 303 pages
The volumes in this continuing series provide a compilation of current techniques and ideas in inorganic synthetic chemistry. Includes inorganic polymer syntheses and preparation of important inorganic solids, syntheses used in the development of pharmacologically active inorganic compounds, small-molecule coordination complexes, and related compounds. Also contains valuable information on transition organometallic compounds including species with metal-metal cluster molecules. All syntheses presented here have been tested.
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absorption acetate acetone acetonitrile acid added dropwise alkyl Anal aneN4 anhydrous anion aqueous bands benzene Calcd carbon carbonyl Chem Chemical chloride chloroform collected by ﬁltration complex compound concentrated cooled copper(l crystalline crystals Department of Chemistry dichloromethane diethyl ether dissolved distilled dried in vacuo extracted ﬁltrate ﬁrst ﬁtted ﬂask ﬂushed Found heated at reﬂux hexane hydrogen infrared Inorg insoluble isomer ligand metal methanol methylcobalamin minutes mixture is stirred mmole mole nitrogen nmr spectrum obtained organic solvents Organomet oxide pentane perchlorate phosphine phthalonitrile porphyrins powder precipitate prepared Procedure I Caution Properties puriﬁed pyridine reagent recrystallized reduced pressure removed residue rhenium rhodium room temperature rotary evaporator round-bottomed ﬂask salt Schlenk singlet slowly sodium solid soluble solvents stable starting material stirring bar sulfate Synth synthesis tetrahydrofuran tion torr Trimethylphosphine tube University vacuum volume washed yellow yield